Abstract

The determination of lead in leaded steel by x-ray spectroscopy is highly dependent on proper surface preparation because of the tendency toward smearing or removal of the lead. A metallographic preparation technique using diamond dust as the abrasive is shown to provide reproducible and accurate results even with appreciable changes in the particle size of the lead. This work is part of a cooperative program with the United States Steel Corporation in the preparation of a leaded-steel spectrochemical standard. Although certain inhomogeneities, both linear and radial, were observed by x-ray spectroscopy in the rods tested, suitable material has been selected for use as the National Bureau of Standards spectroscopic standard.

Surface roughness of stainless-steel mirrors for focusing soft x rays

Valeriy V. Yashchuk, Eric M. Gullikson, Malcolm R. Howells, Steve C. Irick, Alastair A. MacDowell, Wayne R. McKinney, Farhad Salmassi, Tony Warwick, James P. Metz, and Thomas W. Tonnessen
Appl. Opt. 45(20) 4833-4842 (2006)

Spectroscopy of x-ray lasers

R. H. Dixon and R. C. Elton
J. Opt. Soc. Am. B 1(2) 232-238 (1984)

High resolution X-ray spectra of stainless steel foils irradiated by femtosecond laser pulses with ultra-relativistic intensities

M. A. Alkhimova, A. Ya. Faenov, I. Yu. Skobelev, T. A. Pikuz, M. Nishiuchi, H. Sakaki, A. S. Pirozhkov, A. Sagisaka, N. P. Dover, Ko. Kondo, K. Ogura, Y. Fukuda, H. Kiriyama, K. Nishitani, T. Miyahara, Y. Watanabe, S. A. Pikuz, M. Kando, R. Kodama, and K. Kondo
Opt. Express 25(23) 29501-29511 (2017)

Determinations of trace boron in superalloys and steels using laser-induced breakdown spectroscopy assisted with laser-induced fluorescence

Changmao Li, Zhongqi Hao, Zhimin Zou, Ran Zhou, Jiaming Li, Lianbo Guo, Xiangyou Li, Yongfeng Lu, and Xiaoyan Zeng
Opt. Express 24(8) 7850-7857 (2016)

Carbon determination in carbon-manganese steels under atmospheric conditions by Laser-Induced Breakdown Spectroscopy

Timur A. Labutin, Sergey M. Zaytsev, Andrey M. Popov, and Nikita B. Zorov
Opt. Express 22(19) 22382-22387 (2014)