Abstract
The profile of a fine local defect in a periodic surface relief structure is reconstructed from a scattered wave. This defect cannot be imaged with an optical imaging system owing to the diffraction limit, and complicated multiscattering among the high-aspect-ratio grooves and the defect makes it difficult to reconstruct the profile using the scalar diffraction theory. We propose and numerically demonstrate a reconstruction algorithm by applying an efficient vector analysis method—the difference-field boundary element method. We also classify the profile according to the difficulty of reconstruction, which depends on the observation system and the noise level. Finally, this analysis provides the accuracy and limit of reconstruction under the vector diffraction theory.
© 2020 Optical Society of America under the terms of the OSA Open Access Publishing Agreement
1. Introduction
Advances in nanofabrication technology have led to the miniaturization of semiconductor devices. Dust adhesion and contamination during the fabrication process cause defects in the products. Even the slightest fabrication error can cause severe damage to device operation in extremely integrated circuits. Defect detection in products, semiconductor wafers in each fabrication step, and photomasks in the lithography system are necessary to enhance yields. An electron microscope and an atomic-force microscope provide sufficient resolution for defect detection. However, a substantial amount of time is necessary for scanning the entire device. In contrast, while an optical microscope can measure a wide range of wafer surfaces, the resolution of an image is restricted by the diffraction limit. Under the scalar diffraction theory, the amplitude and phase distribution of a light wave just over the sample are proportional to the reflectance and the surface profile of the sample, respectively. The limit of measurement is simply described as the highest spatial frequency in the sample that can be imaged. For example, Abbe’s criterion provides a limit resolution of $\lambda /2$ with the maximum numerical aperture (NA) of a dry objective lens.
Although a microscope cannot produce a sample image, the information on the sample structure can be captured as scattered or diffracted waves. The problem of reconstructing a sample from a scattered wave is called the inverse scattering problem. So far, various methods have been proposed to solve this problem. Optical diffraction tomography can provide a cross-sectional image of the sample with low-refractive-index contrast. In this method, the relationship between sample structure and scattered field is represented as an approximation, such as the Born and Rytov approximation [1–4]. When the sample contains high-refractive-index interfaces, an iterative method is employed. In this approach, we first define an objective function that represents the error between the measured scattered waves from the sample and the computed scattered waves for the estimated structure. The sample structure is then reconstructed to minimize the object function. Some studies have reconstructed a sample profile beyond the diffraction limit. In acoustic engineering, a particle shape has been reconstructed from the phaseless data of a scattered wave [5,6]. In this method, the integral equations provide a scattered field, and a minimum of the object function is found by the Newton method. This approach has been applied to the inverse electromagnetic-field-scattering problem [7,8]. The uniqueness of the results reconstructed from phaseless far-field data has also been discussed [9,10].
Reconstruction of the profiles of a structure on a planar substrate has also been studied. This technique is known as optical diffraction microscopy or optical profilometry. For example, Kress et al. reconstructed the profile of a local protrusion on a perfectly conductive plane with boundary-integral equations of the Helmholtz equation and Newton method [11]. Garnaes et al. determined the grating parameters from diffracted waves and measured them using an atomic-force microscope [12]. Hansen et al. applied a renormalized scalar diffraction theory to determine the grating parameter [13]. Karamehmedović et al. estimated the defect in a finite-sized grating. The scattered wave was computed using the auxiliary source method [14]. They also reconstructed the profile of a platinum submicron wire on a Si substrate using a scattered field expression with an approximated Green’s function [15]. Afifi et al. reconstructed the sample profiles with a rough surface whose height was much less than the illuminating wavelength [16]. Ishikawa et al. identified the nanostructure on a substrate by matching the observed data with the template data containing scattered fields of various structures [17]. Maire et al. reconstructed the shapes of submicron rods on a flat substrate [18]. The scattered fields were computed using a volume-integral equation. This method was also experimentally demonstrated [19]. Zang et al. expanded this approach to three-dimensional reconstruction by introducing the polarization characteristics of the scattered field [20]. Zhang et al. proposed an algorithm for imaging a locally rough surface with boundary-integral equations [21,22].
In this study, we reconstruct a more complicated structure, the profile of a local defect in an infinite number of periodically aligned groove structures. The defect is a deformed groove that can be seen in bio-fabricated devices. Because the groove period and depth are comparable to the illuminating wavelength, strong multiple scattering occurs over the entire device surface. Approximations such as scalar-wave approximation and the Born and Rytov approximations cannot be employed for computing the scattered and diffracted fields and for evaluating the objective function. We have previously proposed the difference-field boundary element method (DFBEM) [23]. The DFBEM computes the scattered wave from the complicated surface relief structure with low computational resources. We arrange the DFBEM for the inverse scattering problem and reconstruct the defect profile of the sample.
Unlike the resolution theory under scalar diffraction approximation, such as Abbe’s criterion and Rayleigh’s criterion, the resolution limit of the iterative method is less discussed. As the studies introduced above have demonstrated, an iterative method can reconstruct a sample profile beyond the resolution limit of an optical imaging system. We also discuss the profile shape that can be reconstructed under the given observation system and noise level. This discussion can be used as a generalized criterion for the reconstruction limit of the iterative method that can be used to estimate if the profile can be reconstructed for various sample shapes.
In the following section, we derive the integral equation of DFBEM for the inverse problem. We also present an optical system to acquire the scattered wave, and its modeling for numerical analysis. In Section 3, we numerically simulate the defect reconstruction. We show the reconstruction results as a relation between the reconstruction accuracy and the observation system conditions such as NA and noise level. Finally, we discuss the limit and accuracy estimation of profile reconstruction.
2. Principle of profile reconstruction
In the reconstruction process, we set an object function that evaluates the error between experimentally observed data of the sample and numerically computed data of the estimated structure. The estimated sample structure is iteratively modified to minimize the objective function. The observed data is acquired by the optical system depicted in Fig. 1. Electromagnetic fields and all structures, including the sample and lenses, are invariant along the $z$-axis. Therefore, we consider only two-dimensional field distribution in the $x$-$y$ plane. The sample is placed so that the surface is on $y = 0$. This optical system is equivalent to an optical microscope. The field at $y = {y_\textrm{o}}{\; }({ > 0} )$ is imaged on the observation line with the objective lens ${\textrm{L}_1}$ and imaging lens ${\textrm{L}_2}$, whose focal lengths are ${F_1}$ and ${F_2}$, respectively. Note that the defect in the sample cannot be imaged clearly because the sample surface is out of focus and the defect is less than the illuminating wavelength, $\lambda $. The defect groove is located on the optical axis, $x = 0$. This alignment is possible by referring to the defocused image of the sample.
The sample is a one-dimensional diffraction grating. All grooves have a rectangular profile with a period T. The groove shape and the period are known parameters. In contrast, the unknown defect profile $y(x )$ is expressed as
where ${\boldsymbol u} = {\left[ {\begin{array}{cccc} {{u_1}}&{{u_2}}& \cdots &{{u_N}} \end{array}} \right]}^{{\textrm{t}}}$ is a structural vector (unknown). The symbol $\textrm{t}$ denotes the vector transposition. ${U_n}(x )$ $({n = 1,2, \cdots N} )$ are the basis functions (known). The estimation of the defect profile is then reduced to a problem of determining the unknown vector ${\boldsymbol u}$.We define the object function as
In the conjugate gradient method, the evaluation of $h({\boldsymbol u} )$ and its gradient
After obtaining ${f_{0p}}$, we can compute $\varDelta {f_1}$ and its normal derivatives $\partial \varDelta {f_1}/\partial n$ on ${C_0}$, ${f_3}$ and $\partial {f_3}/\partial n$ on ${C_1}$, and ${f_3}$ and $\partial {f_3}/\partial n$ on ${C_2}$ by solving the following integral equations.
The variables $({n,l,z} )$ are components of the local coordinate system on each boundary, l is the tangential direction (indicated by arrows on the boundaries in Fig. 2), and n is in the normal direction. In Eqs. (11) and (12), ${G_p}$ is a Green function defined as
In the numerical computation, the integral path C and fields ${\phi _p}$ are discretized with boundary elements. For example, the integral path C is discretized with points ${{\boldsymbol r}_i}$ on $C$. The boundary elements are short straight lines between ${{\boldsymbol r}_i}$ and ${{\boldsymbol r}_{i + 1}}$. The position on the element ${\boldsymbol r^{\prime}}$ is represented by a parameter $s^{\prime}$ ($- 1 \le s^{\prime} \le 1$).
This function removes the high-spatial-frequency and evanescent field, which cannot be propagated through the observation system. The field distribution on the image plane ${\psi _g}({{\boldsymbol u},{\boldsymbol r}_m^{\boldsymbol{\prime}}} )$ $({m ={-} {N_\textrm{o}}, - {N_\textrm{o}} + 1,\; \cdots ,{N_\textrm{o}}} )$ is computed as
The computation of ${\psi _g}({{\boldsymbol u},{\boldsymbol r}_m^{\prime}} )$ from $\varDelta {f_2}({{\boldsymbol u},{{\boldsymbol r}_i}} )$ is a linear operation and can be expressed as
where B is a matrix, and ${{\boldsymbol \psi }_g}$ and $\varDelta {{\boldsymbol f}_2}$ are vectors defined asThe next step computes the gradient of the object function ${\nabla _{\boldsymbol u}}h({\boldsymbol u} )$. The adjoint-variable method [25,26] and a direct derivative can be used for this purpose. In this study, we apply the latter method for the analysis described in Section 4. From Eq. (2), the $l$-th component of ${\nabla _{\boldsymbol u}}h({\boldsymbol u} )$ is
Because the matrix B does not depend on ${\boldsymbol u}$, the derivative of ${\psi _g}({{\boldsymbol u},{r_i}} )$ is given by the derivative of $\varDelta {{\boldsymbol f}_2}({\boldsymbol u} )$
According to Eq. (18), the derivative of the integral operator for ${C_2}$ is
Variation in ${u_l}$ changes the defect shape $y(x )$, which leads to the displacement of the y-coordinate of the element nodes on ${C_2}$, as well as the position in the boundary element ${\boldsymbol r}({s^{\prime}} )$ and the element length ${L_i}$. The specific expressions for the derivatives of ${L_i}$, ${G_p}$, and $\partial {G_p}/\partial n^{\prime}$ are described in Ref. [8]. The derivatives of $\varDelta {\phi _1}$ and ${\phi _3}$ are also required to compute Eq. (28). These parameters are provided by solving the derivatives of Eqs. (5)–(10):
The terms on the left-hand sides of Eqs. (30)–(35) are the product of the coefficients and unknown parameters $\partial \phi /\partial {u_l}$; the right-hand sides are constant terms. When solving as a set of simultaneous equations numerically, the coefficient matrix does not depend on l. Hence, $\partial \phi /\partial {u_l}$ for each l can be efficiently solved by the LU decomposition of the coefficient matrix.
3. Reconstruction simulation
The reconstruction process was validated through numerical simulation. We prepared the observation data ${\psi _e}({\boldsymbol r} )$ by numerical simulation, and the defect profile was reconstructed from ${\psi _e}({\boldsymbol r} )$ according to the process described in Section 2. The sample structure is Fig. 3(a) Profile of the sample grating. (b) Profile of the initial guess.illustrated in Fig. 3(a). Hereafter, all parameters of length, such as the dimensions of the sample shape and the sampling interval of the field, are normalized by the illuminating wavelength, $\lambda $. As long as the ratios of these parameters to $\lambda $ and the refractive indices are unchanged, the results also remain unchanged, regardless of the wavelength band. The period of the groove $T = 1.2\lambda $, and the width and depth of the groove are $0.5T$ and $0.3T$, respectively. The structural vector of the sample is represented by a four-dimensional vector:
Since we know that the defect position is on the optical axis ($x = 0$), the defect region is $- T/4 \le x \le T/4$.
In the computation of ${\psi _e}({\boldsymbol r} )$ and the reconstruction process, the lengths of the boundary elements on ${C_0}$ and ${C_1}$ are set to be less than $T/10$. On ${C_2}$, it is set to $T/40$ such that the fine shape can be accurately reflected in the computed result. The refractive indices ${n_1}$, ${n_2}$, and ${n_3}$ are set to 1.5, 1.0, and 1.5, respectively. The incident angle of the illumination is set to $\theta = 0^\circ $. The object plane ${y_\textrm{o}}$ of the optical imaging system is set to ${y_\textrm{o}} = T$. The field distribution on the object plane is discretized with an interval of $0.05T$. The focal lengths ${F_1}$ and ${F_2}$ are set to $9.0 \times {10^3}T$ and $3.6 \times {10^5}T$, respectively. The NA is varied from 0.05–0.95. The field distribution on the image plane is discretized with an interval of $10T.$ Assuming that the observed data ${\psi _e}({{{\boldsymbol r}_i}} )$ contains noise in the actual measurement, normal random numbers with the variance of ${\sigma ^2}$ are added to the real and imaginary parts of ${\psi _e}({{{\boldsymbol r}_i}} )$. For example, when we set a noise level of $x$%, $\sigma $ for the real part is $0.01x\textrm{Re}[{{\psi_e}({{{\boldsymbol r}_i}} )} ]$, and that for the imaginary part is $0.01x\textrm{Im}[{{\psi_e}({{{\boldsymbol r}_i}} )} ]$.
The reconstruction process was performed by the conjugate gradient method with an initial guess of ${\boldsymbol u} = \mathbf{0}$, as illustrated in Fig. 3(b). After computing the conjugate gradient from ${\nabla _{\boldsymbol u}}h({\boldsymbol u} )$, we found an ${\boldsymbol u}$ that provides the minimum $h({\boldsymbol u} )$ in the direction of the conjugate gradient with a golden-section search. This process was iteratively performed in 20 steps. The reconstruction process was performed ten times, while changing the seed of the random numbers. The results were evaluated by field error ${E_f}$ and structural error ${E_s}$ as follows.
The results for each NA and noise level are plotted in Fig. 4. The field error was normalized to that of the initial guess, $E_f^{(0 )}$. The reconstructed defect profiles for some parameters are illustrated in Fig. 5. The exact defect profile is reconstructed for a noise level of 0%, regardless of the NA. When the noise level is more than 0%, the reconstruction accuracy decreases with an decrease in the NA. For example, the noise level must be less than 0.5% and the NA must be larger than 0.1 to achieve ${E_s}$ less than 10%. ${E_s}$ less than 1% can be achieved when the noise level is not more than 0.1%.
4. Discussion on the limit of reconstruction
We discuss the limits of the defect shape that can be reconstructed by the procedure in this study, so as to estimate the potential of reconstruction for various types of defect shapes. An accurate reconstruction result can be achieved when the information on the defect shape is transmitted to the observation line through the optical system. For example, when the defect is deformed to a certain shape, but the field on the observation line varies less than the noise level, the deformation cannot be detected. To discuss quantitatively, we derive a relationship between the variation in defect shape and the variation in field on the observation line. We approximate the small variation in the field ${{\boldsymbol \psi }_g}({\boldsymbol u} )$ because of the variation in defect shape $\varDelta {\boldsymbol u}$ as
The matrices W and V are real orthogonal matrices, that is, ${\boldsymbol w}_n^\textrm{t}{{\boldsymbol w}_m} = {\boldsymbol v}_n^\textrm{t}{{\boldsymbol v}_m} = {\delta _{nm}}$, where ${\delta _{nm}}$ is a Kronecker delta. S is a real diagonal matrix whose $({n,n} )$ components ${s_n}$ (singular value) are arranged in descending order $({{s_n} \ge {s_{n + 1}}} )$. We define another structural vector ${\boldsymbol u^{\prime}}$ and the base functions $U_n^{\prime}(x )$ as
where ${V_{mn}}$ is the $({m,n} )$ component of V. A small variation in the defect shape $\varDelta y(x )$ is expressed using the components of $\varDelta {\boldsymbol u^{\prime}}({ \equiv {V^\textrm{t}}\varDelta {\boldsymbol u}} )$ as Finally, ${{\boldsymbol \psi }_g}({{\boldsymbol u} + \varDelta {\boldsymbol u}} )$ is represented asBased on the above discussion, we estimate the reconstruction accuracy from the singular values and the noise level of the observed data, ${\psi _e}({{{\boldsymbol r}_i}} )$. In the following discussion, we do not consider the case of converging the local minimum in the searching algorithm on the conjugate gradient method. We can avoid such a case by restarting the reconstruction process by changing the initial guess of ${\boldsymbol u}$. Here, we assume that the object function is minimal at ${{\boldsymbol u}_0} + \varDelta {\boldsymbol u}$, which is slightly shifted by $\varDelta {\boldsymbol u}$ from the sample shape ${{\boldsymbol u}_0}$ owing to the noise in the observed data. From Eqs. (2) and (50), the object function $h({{{\boldsymbol u}_0} + \varDelta {\boldsymbol u}} )$ is expressed as
We computed ${\sigma _{u,m}}$ for each component of $\varDelta {\boldsymbol u^{\prime}}$ at ${\boldsymbol u}_0^{\boldsymbol{\prime}}$. Because the noise in ${\psi _e}({{{\boldsymbol r}_n}} )$ (noise level of $x$%) is generated from a normal random number such that the variance of ${\psi _e}({{{\boldsymbol r}_n}} )$ is given by
The variance ${\sigma _{u,m}}$ calculated from Eqs. (57) and (58) is plotted in Fig. 8. We also plot the actual error $|{u_m^{\prime} - u_{0m}^{\prime}} |$ obtained by the reconstruction process described in Section 3. The ${\sigma _{u,m}}$ is located near the center of the distribution of the reconstruction results, and is valid as an estimated accuracy of $|{u_m^{\prime} - u_{0m}^{\prime}} |$.
As an application, we evaluated ${\sigma _{u,m}}$ for other sample structures (different refractive-index contrast and different aspect ratio of the surface relief structure). First, the refractive index ${n_1}({ = {n_3}} )$ was varied from 1.5 to 2.5 or 3.5, while ${n_2}({ = 1.0} )$ remained unchanged. The NA and the noise level were set to 0.6 and 1.0%, respectively. As listed in Table 1, ${\sigma _{u,3}}$ and ${\sigma _{u,4}}$ decrease with increasing the contrast, ${n_1}/{n_2}$. As Eq. (57) indicates, the smaller ${\sigma _{u,m}}$ is due to the greater singular value, ${s_m}$. The singular value, ${s_m}$ becomes greater when the intensity of the field difference for structural variation of $u_m^{\prime}$ is larger. In general, the intensity of the field difference for $u_3^{\prime}$ and $u_4^{\prime}$ is small because of destructive interference between neighboring negative and positive sources as plotted in Figs. 7(c) and 7(d). However, in a higher refractive-index material, the wavelength becomes shorter, and the interval between the negative and positive source is relatively extended. As a result, the destructive interference diminishes, and the field difference becomes larger.
Second, we evaluated ${\sigma _{u,m}}$ for different aspect ratio of the sample. The groove depth d was varied from $0.1T$ to $2.0T$, while the groove width ($0.5T$) remained unchanged (the aspect ratio ranging from 0.2 to 4.0). The defect depth was also varied in proportion to d;
Finally, we extended the dimension of the structural vector from four to twelve to investigate the limit of reconstruction. The basis function is defined by Eq. (37). Because the structural vector can express a finer (higher spatial frequency) profile, the defect surface (boundary ${C_2}$) was discretized by 40 elements. The base function $U_n^{\prime}(x )\; ({ - T/4 \le x \le T/4} )$ and the singular values are plotted in Fig. 11. The base functions $U_1^{\prime}(x )$ and $U_2^{\prime}(x )$, whose singular values are more than 75, have two peaks near the edges $({x ={\pm} T/4} )$. The shapes are mirror-symmetric for $U_1^{\prime}(x )$ and anti-symmetric for $U_2^{\prime}(x )$ with respect to a line $x = 0$. Because these functions represent a structural variation at two points apart from each other, ranging near the Abbe’s limit $T/2$, they can be detected as a strong signal as a variation of ${{\boldsymbol \psi }_e}$. $U_4^{\prime}(x )$ represents a variation whose depth in the defect is uniformly changed. As depicted in Fig. 7(a), this component can also be detected as a strong signal. $U_5^{\prime}(x )$ and $U_6^{\prime}(x )$ are similar to the triangular functions. Considering that the incident wave reflects on their linear slope, the reflected wave is detected as a strong signal on the observed line. The estimated ${\sigma _{u,m}}$ values are plotted in Fig. 12. The estimated error exponentially increases with m, and finally, ${\sigma _{u,12}}$ is ${10^4}$ times larger than the first component ${\sigma _{u,1}}$. As for $m > 10$ with a noise level of 0.1%, and for $m > 7$ with a noise level of 5%, ${\sigma _{u,m}}$ is larger than the groove depth, $0.3T$. Reconstruction of these components is virtually impossible under these conditions.
The reconstruction algorithm can be applied to other optical measurement systems if we can compute the system output, ${\psi _g}({\boldsymbol r} )$, from the scattered wave $\varDelta {f_2}({\boldsymbol r} )$. If this relationship is expressed by a matrix as Eq. (23), we can also estimate the reconstruction accuracy. For example, the optical system depicted in Fig. 1 is replaced with a scanning near-field optical microscope, which provides high-resolution images of samples by acquiring the evanescent field on the sample surface by a scanning probe. For simplicity, the microscope system is approximated by a spatial filter. The matrix B in Eq. (23) was configured by Fourier and inverse Fourier transform and a low-pass filter whose cut-off spatial frequency is $NA/\lambda $, where $NA$ corresponds to the numerical aperture of the objective lens. When $NA > 1$, ${\psi _g}({{\boldsymbol u},{\boldsymbol r}} )$ and ${\psi _e}({{{\boldsymbol r}_i}} )$ contain the evanescent field. The reconstruction accuracy, ${\sigma _{u,m}}$ at ${\boldsymbol u}_0^{\boldsymbol{\prime}}$ for $NA < 10$ is plotted in Fig. 13. The estimated ${\sigma _{u,m}}$ slowly decreases with increasing NA. Because this sample, which consists of a transparent dielectric material, produces little evanescent field (see the defect surface in Fig. 7(d)), the effect on improving the accuracy is small.
5. Conclusion
We developed a reconstruction process for local defect in a periodic surface relief structure. The reconstruction process applies an optimization algorithm using the conjugate gradient method. We arranged the DFBEM boundary-integral equations for efficient computation of the objective function and its gradient. Because discretization in the region using mesh and grid is not necessary, mesh regeneration and grid resampling are also not necessary when the estimated defect shape is updated in the reconstruction process. The integral equations also represent a direct relationship between the deformation of the defect profile and the observed field data. This relationship leads to the precise analysis of possible reconstruction of a fine defect profile.
Regarding the numerical simulation of defect reconstruction, we found that the reconstruction for a fine defect profile, whose spatial frequency is beyond the Abbe’s limit, can be achieved with the existence of noise in the observed data. For a general case of profile reconstruction, we classified a profile shape that can be easily or hardly reconstructed using singular value decomposition, and also quantified the degree of difficulty of reconstruction to estimate the reconstruction accuracy. The easily reconstructed profiles are those whose depth is uniformly varied, which are deformed at two positions apart from each other, and whose slope is changed. The hardly reconstructed profile fluctuates in a narrow region. The latter hardly contributes to the field distribution on the observation line, and the signal is easily buried in the noise floor. Unlike the scalar diffraction theory, it is not simply classified by the spatial frequency of the sample. Even when the spatial frequency of the defect profile is beyond the diffraction limit, the scattered wave can propagate and be detected through an optical imaging system.
The observed data that is referred to in the reconstruction contains phase information of the scattered field. For more practical cases, reconstruction from phaseless data that consists of the intensity or amplitude of a field can also be achieved by only arranging the objective function. We will analyze the limit of reconstruction under this condition of observation is our future work.
Funding
Japan Society for the Promotion of Science (19K12012).
Disclosures
The authors declare no conflicts of interest.
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