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Optica Publishing Group
  • Applied Spectroscopy
  • Vol. 21,
  • Issue 3,
  • pp. 183-184
  • (1967)

Microcell for Nuclear Magnetic Resonance Analyses

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Abstract

The use of a commercially available all-glass spherical sample-chamber microcell in combination with a time-averaging computer for nuclear magnetic resonance (NMR) analyses of microsamples has recently been reported. Brame has described a technique for trapping small gas-chromatographically isolated samples directly in such an all-glass NMR microcell. A somewhat different, easily fabricated microcell has been constructed and tested in our laboratories with excellent results. The design is a modification of a cell first described by Frei and Niklaus.

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