Review on infrared nanospectroscopy of natural 2D phyllosilicates

Raphaela de Oliveira; Raphaela de Oliveira; Alisson R. Cadore; Raul O. Freitas; Ingrid D. Barcelos

doi:10.1364/JOSAA.482518

Journal of the Optical Society of America A
Vol. 40,
Issue 4,
pp. C157-C168
(2023)
•https://doi.org/10.1364/JOSAA.482518

Review on infrared nanospectroscopy of natural 2D phyllosilicates

Raphaela de Oliveira, Alisson R. Cadore, Raul O. Freitas, and Ingrid D. Barcelos

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Raphaela de Oliveira, Alisson R. Cadore, Raul O. Freitas, and Ingrid D. Barcelos, "Review on infrared nanospectroscopy of natural 2D phyllosilicates," J. Opt. Soc. Am. A 40, C157-C168 (2023)

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Abstract

Phyllosilicates have emerged as a promising class of large bandgap lamellar insulators. Their applications have been explored from the fabrication of graphene-based devices to 2D heterostructures based on transition metal dichalcogenides with enhanced optical and polaritonics properties. In this review, we provide an overview of the use of infrared (IR) scattering-type scanning near-field optical microscopy (s-SNOM) for studying nano-optics and local chemistry of a variety of 2D natural phyllosilicates. Finally, we bring a brief update on applications that combine natural lamellar minerals into multifunctional nanophotonic devices driven by electrical control.

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Group	Specimen	Chemical Formula	Frequency ( ${c m}^{- 1}$ )	Assignment
Mica	Muscovite	${K A l}_{2} (A l, {S i}_{3}) O_{10} (O H)_{2}$	1080 831 920	Si–O stretching Al–O stretching mixed Al–OH/Al–O–Al stretching and Si–O–Si/Si–O–Al stretching
	Phlogopite	${K M g}_{3} ({A l S i}_{3}) O_{10} (O H)_{2}$	472 508 682 750 809 851 960 1001 1062	$∥$ Si-O stretching $∥$ Si-O stretching Si-O-Mg stretching $∥$ Si/Al-O-Si stretching $∥$ Si/Al-O-Si stretching $⊥$ Si/Al-O stretching $∥$ Si-O stretching $∥$ Si-O stretching Si-O stretching
Chlorite	Clinochlore	${M g}_{5} A l ({A l S i}_{3}) O_{10} (O H)_{8}$	420 445 470 492 521 680 811 987 1023	(Fe, Mg)-O-Si or Al-O-Si bending $∥$ Si–O bending metal-OH translation (Fe, Mg)-O-Si or Al-O-Si bending (Fe, Mg)-O-Si or Al-O-Si bending metal-OH libration Al–O stretching $∥$ Si–O stretching $∥$ Si–O stretching
Clay	Talc	${M g}_{3} {S i}_{4} O_{10} (O H)_{2}$	670 690 990 1010	$∥$ OH libration OH libration $∥$ Si–O stretching $⊥$ Si–O stretching
Serpentine	Antigorite	${M g}_{3} {S i}_{2} O_{5} (O H)_{4}$	666 960 990 1025	Si-O bending Si–O stretching Si–O stretching Si-O stretching

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Journal of the Optical Society of America A